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ISSN 1998-9539

Microwave-Assisted Synthesis and Characterization of Carba- and Triazolehemiporphyrazines with Camphorapyrazine Fragments

Aleksandra S. Kuznetsova,a@1 Mikhail K. Islyaikin,a@2 and Tomas Torresa,b
aIRLoN, Research Institute of Macroheterocycles, Department of Fine Organic Synthesis, Ivanovo State University of Chemistry and Technology, 153000 Ivanovo, Russia
bDepartamento de Química Orgánica, Universidad Autónoma de Madrid, Cantoblanco, 28049 Madrid, Spain
@1Corresponding author E-mail:
@2Corresponding author E-mail:
DOI: 10.6060/mhc210336k
Macroheterocycles 2021 14(1) 65-69
Dedicated to the memory of Prof. Larisa G. Tomilova
A series of new hemiporphyrazines bearing camphorapyrazine fragments were synthesized using microwave assisted solvent-free protocol by interaction of m-phenylenediamine, 1(H)- or 1-dodecyl-3,5-diamino-1,2,4-triazole with racemic mixture, R-(+)- or S-(‑)-camphoradicyanopyrazines. The obtained macroheterocycles were characterized by mass spectrometry, UV-Vis, IR, 1H and 13C NMR spectroscopy and elemental analysis data.


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