Synthesis and Properties of Macroheterocyclic Compounds of ABAB-Type with tert-Butylpyrrolepyrazine Fragments

Mikhail G. Stryapan, Svetlana V. Efimova, Oscar I. Koifman, and Mikhail K. Islyaikin^@

Ivanovo State University of Chemistry and Technology, Friedrich Engels Pr-t, 7, Ivanovo, 153000, Russia

^@Corresponding author E-mail: islyaikin@isuct.ru

DOI: 10.6060/mhc2010.1.38

Macroheterocycles 2010 3(1) 38-40

New representatives of macroheterocyclic compounds of ABAB-type were synthezised by condensation of m-phenylenediamine or 2,6-diaminopyridine (A) with 5-tert-butyl-2,3-dicyanopyrazine (B) in nBuOH. These compounds were characterizised by UV-vis, IR, 1H NMR spectroscopies, mass-spectrometry and elemental analysis.

References:

Click here to expand or collapse this section

1. Elvidge J.A., Linstead R.P. J. Chem. Soc. 1952, 20, 5008-5012.
http://dx.doi.org/10.1039/jr9520005008

2. Campbel J. B. Pat. 2765308 (USA) 1956.

3. Rodríguez-Morgade M.S., Gema de la Torre, Torres T. Design and Synthesis of Low-Symmetry Phthalocyanines and Related Systems, in The Porphyrin Handbook (Kadish K.M., Smith K.M., Guilard R., Eds.) Amsterdam, Boston, London, New York, Oxford, Paris, San Diego, San Francisco, Singapore, Sydney, Tokyo: Academic Press 2003, Vol. 15, 125–160.
http://dx.doi.org/10.1016/B978-0-08-092389-5.50009-2

4. Islyaikin M.K., Danilova E.A., RomanenkoYu.V., Khelevina O.G., Lomova T.N. Synthesis, Structure Peculiarities and Biological Properties of Macroheterocyclic Compounds, in Chemical Processes with Participation of Biological and Related Compounds. (Lomova T.N., Zaikov G.E., Eds.) BRILL, Leiden-Boston 2008, 219-270.

5. Dini D., Calvete M.J.F., Hanack M., Amendolab V., Meneghetti M. Chem. Commun. 2006, 22, 2394-2396.
http://dx.doi.org/10.1039/b601591c

6. Campaci F., Campestrini S. J. Mol. Catalysis A: Chemical 1999, 140, 121-130.
http://dx.doi.org/10.1016/S1381-1169(98)00236-2

7. Avanzino S. Pat. 7141482 (USA) 2006.

8. Fernánrez-Lazáro F., Torres T., Hauschel B., Hanack M. Chem. Rev. 1998, 98, 563-576.
http://dx.doi.org/10.1021/cr970002a

9. Islyaikin M.K., Danilova E.A. Russ. Chem. Bull., Int. Ed. 2007, 5, 689-706.
http://dx.doi.org/10.1007/s11172-007-0107-z

10. Neustroeva N.R., Kulikov M.A., Vorob'evYu.G., Smirnov R.P. Zh. Obshch. Khim. 1999, 69, 1836-1838 (in Russ.).

11. Danilova E.A., Islyaikin M.K. Synthesis and Properties of tert-ButylsubstitutedMacroheterocyclic Compounds and their Metal Complexes, in UspekhiKhimiiPorfirinov (Advances in Porphyrin Chemistry) (Golubchikov O.A., Ed.) St. Petersburg: NII KhimiiSPbGU 2004, Vol. 4, 356-375 (in Russ.).

12. Islyaikin M.K., Mayzlish V.E., Borodkin V.F. Izv. Vyssh. Uchebn. Zaved.,Khim. Khim. Tekhnol. 1979, 22, 152-154.

13. Rodriguez-Morgade M.S., Pantos G.D., Caballero E., Sessler J.L., Torres T. Macroheterocycles 2008, 1, 40-43.
http://dx.doi.org/10.6060/mhc2008.1.40

Attachment	Size
MHC2010_t03n01_38-40.pdf	445.19 KB

Журнал "Макрогетероциклы"

Navigation

Languages

News

Search